Information card for entry 4085245

Structure parameters

• Formula: C32 H64 K2 N2 Si4
• Calculated formula: C32 H64 K2 N2 Si4
• SMILES: C(C)(C)(C)[Si](C)(C)[N]1([Si](C)(C)C)[K][N]([Si](C)(C)C(C)(C)C)([Si](C)(C)C)[K]1.c1cc(ccc1)C.c1cc(ccc1)C
• Title of publication: Homoleptic Trigonal Planar Lanthanide Complexes Stabilized by Superbulky Silylamide Ligands
• Authors of publication: Goodwin, Conrad A. P.; Joslin, Kristian C.; Lockyer, Selena J.; Formanuik, Alasdair; Morris, Gareth A.; Ortu, Fabrizio; Vitorica-Yrezabal, Iñigo. J.; Mills, David P.
• Journal of publication: Organometallics
• Year of publication: 2015
• Journal volume: 34
• Journal issue: 11
• Pages of publication: 2314
• a: 9.1887 ± 0.0008 Å
• b: 11.1315 ± 0.001 Å
• c: 11.3719 ± 0.0009 Å
• α: 73.069 ± 0.007°
• β: 68.473 ± 0.008°
• γ: 78.927 ± 0.007°
• Cell volume: 1030.37 ± 0.17 ų
• Cell temperature: 150.05 ± 0.13 K
• Ambient diffraction temperature: 150.05 ± 0.13 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0812
• Residual factor for significantly intense reflections: 0.0537
• Weighted residual factors for significantly intense reflections: 0.0917
• Weighted residual factors for all reflections included in the refinement: 0.1095
• Goodness-of-fit parameter for all reflections included in the refinement: 1.088
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No