Information card for entry 4085246

Structure parameters

• Formula: C24 H60 K2 N2 Si4
• Calculated formula: C24 H60 K2 N2 Si4
• Title of publication: Homoleptic Trigonal Planar Lanthanide Complexes Stabilized by Superbulky Silylamide Ligands
• Authors of publication: Goodwin, Conrad A. P.; Joslin, Kristian C.; Lockyer, Selena J.; Formanuik, Alasdair; Morris, Gareth A.; Ortu, Fabrizio; Vitorica-Yrezabal, Iñigo. J.; Mills, David P.
• Journal of publication: Organometallics
• Year of publication: 2015
• Journal volume: 34
• Journal issue: 11
• Pages of publication: 2314
• a: 10.3328 ± 0.0018 Å
• b: 11.995 ± 0.002 Å
• c: 15.134 ± 0.003 Å
• α: 89.235 ± 0.014°
• β: 89.606 ± 0.014°
• γ: 69.549 ± 0.016°
• Cell volume: 1757.4 ± 0.6 ų
• Cell temperature: 150.01 ± 0.13 K
• Ambient diffraction temperature: 150.01 ± 0.13 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.2429
• Residual factor for significantly intense reflections: 0.1135
• Weighted residual factors for significantly intense reflections: 0.2235
• Weighted residual factors for all reflections included in the refinement: 0.2831
• Goodness-of-fit parameter for all reflections included in the refinement: 1.025
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No