Information card for entry 4085943

Structure parameters

• Formula: C83 H76 Cl6 Co4 N2 O8 P4 Si2
• Calculated formula: C83 H76 Cl6 Co4 N2 O8 P4 Si2
• Title of publication: Synthesis and Properties of New Dimeric η2-Diyne Complexes of Cobalt Linked through an Azobenzene Ligand
• Authors of publication: Moreno, Consuelo; Arnanz, Avelina; Medina, Rosa-María; Macazaga, María-José; Pascual, Mario; García-Frutos, Eva M.; Martínez-Gimeno, Esther; Marcos, María-Luisa
• Journal of publication: Organometallics
• Year of publication: 2015
• Journal volume: 34
• Journal issue: 12
• Pages of publication: 2971
• a: 12.1496 ± 0.0016 Å
• b: 15.407 ± 0.002 Å
• c: 23.676 ± 0.003 Å
• α: 90°
• β: 102.432 ± 0.007°
• γ: 90°
• Cell volume: 4328 ± 1 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0726
• Residual factor for significantly intense reflections: 0.0467
• Weighted residual factors for significantly intense reflections: 0.1128
• Weighted residual factors for all reflections included in the refinement: 0.1266
• Goodness-of-fit parameter for all reflections included in the refinement: 1.032
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No