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Information card for entry 4086364
Preview
Coordinates | 4086364.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C31 H59 Cl6 N O Os P2 |
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Calculated formula | C31 H59 Cl6 N O Os P2 |
SMILES | [OsH]([P](C(C)C)(C(C)C)C(C)C)([P](C(C)C)(C(C)C)C(C)C)(Cl)(Cl)#CCCCNC(=O)c1ccccc1.ClCCl.ClCCl |
Title of publication | Amide-Directed Formation of Five-Coordinate Osmium Alkylidenes from Alkynes. |
Authors of publication | Casanova, Noelia; Esteruelas, Miguel A.; Gulías, Moisés; Larramona, Carmen; Mascareñas, José L; Oñate, Enrique |
Journal of publication | Organometallics |
Year of publication | 2016 |
Journal volume | 35 |
Journal issue | 2 |
Pages of publication | 91 - 99 |
a | 15.774 ± 0.004 Å |
b | 13.012 ± 0.003 Å |
c | 20.173 ± 0.005 Å |
α | 90° |
β | 105.651 ± 0.004° |
γ | 90° |
Cell volume | 3987 ± 1.7 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 7 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0579 |
Residual factor for significantly intense reflections | 0.0356 |
Weighted residual factors for significantly intense reflections | 0.0652 |
Weighted residual factors for all reflections included in the refinement | 0.0719 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.997 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4086364.html
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