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Information card for entry 4086365
Preview
Coordinates | 4086365.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C22 H48 Cl2 Os P2 |
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Calculated formula | C22 H48 Cl2 Os P2 |
SMILES | C(=C(C)C)=[Os]([P](C(C)C)(C(C)C)C(C)C)(Cl)([P](C(C)C)(C(C)C)C(C)C)Cl |
Title of publication | Amide-Directed Formation of Five-Coordinate Osmium Alkylidenes from Alkynes. |
Authors of publication | Casanova, Noelia; Esteruelas, Miguel A.; Gulías, Moisés; Larramona, Carmen; Mascareñas, José L; Oñate, Enrique |
Journal of publication | Organometallics |
Year of publication | 2016 |
Journal volume | 35 |
Journal issue | 2 |
Pages of publication | 91 - 99 |
a | 21.184 ± 0.003 Å |
b | 9.6719 ± 0.0013 Å |
c | 16.227 ± 0.002 Å |
α | 90° |
β | 125.504 ± 0.002° |
γ | 90° |
Cell volume | 2706.6 ± 0.6 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 5 |
Space group number | 15 |
Hermann-Mauguin space group symbol | C 1 2/c 1 |
Hall space group symbol | -C 2yc |
Residual factor for all reflections | 0.0231 |
Residual factor for significantly intense reflections | 0.0213 |
Weighted residual factors for significantly intense reflections | 0.0477 |
Weighted residual factors for all reflections included in the refinement | 0.0484 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.039 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4086365.html
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