Crystallography Open Database

Information card for entry 4086761

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Coordinates	4086761.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C83 H127 O4 Si2 W2
Calculated formula	C83 H127 O4 Si2 W2
Title of publication	A Silylyne Tungsten Complex Having an Eind Group on Silicon: Its Dimer‒Monomer Equilibrium and Cycloaddition Reactions with Carbodiimide and Diaryl Ketones
Authors of publication	Takashi Yoshimoto; Hisako Hashimoto; Naoki Hayakawa; Tsukasa Matsuo; Hiromi Tobita
Journal of publication	Organometallics
Year of publication	2016
Pages of publication	3444 - 3447
a	13.7165 ± 0.0008 Å
b	14.2405 ± 0.0006 Å
c	20.985 ± 0.0015 Å
α	83.3105 ± 0.0015°
β	88.5806 ± 0.0019°
γ	76.323 ± 0.003°
Cell volume	3955.6 ± 0.4 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0602
Residual factor for significantly intense reflections	0.044
Weighted residual factors for significantly intense reflections	0.1088
Weighted residual factors for all reflections included in the refinement	0.1194
Goodness-of-fit parameter for all reflections included in the refinement	1.171
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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