Crystallography Open Database

Information card for entry 4086762

Preview

Coordinates	4086762.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C29 H22 B F15 N2
Calculated formula	C29 H22 B F15 N2
Title of publication	A Silylyne Tungsten Complex Having an Eind Group on Silicon: Its Dimer‒Monomer Equilibrium and Cycloaddition Reactions with Carbodiimide and Diaryl Ketones
Authors of publication	Takashi Yoshimoto; Hisako Hashimoto; Naoki Hayakawa; Tsukasa Matsuo; Hiromi Tobita
Journal of publication	Organometallics
Year of publication	2016
Pages of publication	3444 - 3447
a	9.3068 ± 0.0003 Å
b	11.0982 ± 0.0005 Å
c	28.5353 ± 0.001 Å
α	90°
β	94.9836 ± 0.0006°
γ	90°
Cell volume	2936.23 ± 0.19 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.1215
Residual factor for significantly intense reflections	0.0937
Weighted residual factors for significantly intense reflections	0.1908
Weighted residual factors for all reflections included in the refinement	0.2076
Goodness-of-fit parameter for all reflections included in the refinement	1.268
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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