Information card for entry 4087065
Formula |
C50 H64 Cl2 N6 O Sn2 |
Calculated formula |
C50 H56 Cl2 N6 O Sn2 |
Title of publication |
Synthesis and Reactivity of Intramolecularly NHC-Stabilized Germylenes and Stannylenes |
Authors of publication |
Paul, Daniel; Heins, Frederik; Krupski, Sergei; Hepp, Alexander; Daniliuc, Constantin G.; Klahr, Kevin; Neugebauer, Johannes; Glorius, Frank; Hahn, F. Ekkehardt |
Journal of publication |
Organometallics |
Year of publication |
2017 |
a |
8.274 ± 0.0004 Å |
b |
12.232 ± 0.0006 Å |
c |
49.393 ± 0.002 Å |
α |
90° |
β |
94.804 ± 0.001° |
γ |
90° |
Cell volume |
4981.4 ± 0.4 Å3 |
Cell temperature |
153 ± 2 K |
Ambient diffraction temperature |
153 ± 2 K |
Number of distinct elements |
6 |
Space group number |
14 |
Hermann-Mauguin space group symbol |
P 1 21/n 1 |
Hall space group symbol |
-P 2yn |
Residual factor for all reflections |
0.0771 |
Residual factor for significantly intense reflections |
0.0485 |
Weighted residual factors for significantly intense reflections |
0.1022 |
Weighted residual factors for all reflections included in the refinement |
0.1113 |
Goodness-of-fit parameter for all reflections included in the refinement |
1.105 |
Diffraction radiation wavelength |
0.71073 Å |
Diffraction radiation type |
MoKα |
Has coordinates |
Yes |
Has disorder |
Yes |
Has Fobs |
No |
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