Information card for entry 4087066

Structure parameters

• Formula: C30 H40 Ge N3 O
• Calculated formula: C30 H40 Ge N3 O
• Title of publication: Synthesis and Reactivity of Intramolecularly NHC-Stabilized Germylenes and Stannylenes
• Authors of publication: Paul, Daniel; Heins, Frederik; Krupski, Sergei; Hepp, Alexander; Daniliuc, Constantin G.; Klahr, Kevin; Neugebauer, Johannes; Glorius, Frank; Hahn, F. Ekkehardt
• Journal of publication: Organometallics
• Year of publication: 2017
• a: 13.0226 ± 0.0004 Å
• b: 15.0573 ± 0.0005 Å
• c: 14.4071 ± 0.0005 Å
• α: 90°
• β: 96.067 ± 0.001°
• γ: 90°
• Cell volume: 2809.2 ± 0.16 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0311
• Residual factor for significantly intense reflections: 0.0247
• Weighted residual factors for significantly intense reflections: 0.0563
• Weighted residual factors for all reflections included in the refinement: 0.0592
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No