Information card for entry 4088175

Structure parameters

• Chemical name: Tetraethylammonium bis(?2-hydrido)-tridecacarbonyl-arsenic-tetra-iron
• Formula: C21 H22 As Fe4 N O13
• Calculated formula: C21 H22 As Fe4 N O13
• Title of publication: Transformations in Transition-Metal Carbonyls Containing Arsenic: Exploring the Chemistry of [Et4N]2[HAs{Fe(CO)4}3] in the Search for Single-Source Precursors for Advanced Metal Pnictide Materials
• Authors of publication: Schipper, Desmond E.; Young, Benjamin E.; Whitmire, Kenton H.
• Journal of publication: Organometallics
• Year of publication: 2016
• Journal volume: 35
• Journal issue: 4
• Pages of publication: 471
• a: 18.3684 ± 0.0011 Å
• b: 17.8643 ± 0.0012 Å
• c: 18.3983 ± 0.0013 Å
• α: 90°
• β: 100.377 ± 0.002°
• γ: 90°
• Cell volume: 5938.4 ± 0.7 ų
• Cell temperature: 173 K
• Ambient diffraction temperature: 173 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0829
• Residual factor for significantly intense reflections: 0.0437
• Weighted residual factors for significantly intense reflections: 0.0916
• Weighted residual factors for all reflections included in the refinement: 0.1194
• Goodness-of-fit parameter for all reflections included in the refinement: 1.176
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No