Information card for entry 4088176

Structure parameters

• Chemical name: Tetraethylammonium (?2-carbonyl)-(?2-hydrido)-(?4-arsenic)-pentadecacarbonyl-tri-iron-manganese
• Formula: C23 H21 As Fe3 Mn N O15
• Calculated formula: C23 H21 As Fe3 Mn N O15
• Title of publication: Transformations in Transition-Metal Carbonyls Containing Arsenic: Exploring the Chemistry of [Et4N]2[HAs{Fe(CO)4}3] in the Search for Single-Source Precursors for Advanced Metal Pnictide Materials
• Authors of publication: Schipper, Desmond E.; Young, Benjamin E.; Whitmire, Kenton H.
• Journal of publication: Organometallics
• Year of publication: 2016
• Journal volume: 35
• Journal issue: 4
• Pages of publication: 471
• a: 12.62 ± 0.008 Å
• b: 14.615 ± 0.009 Å
• c: 17.279 ± 0.011 Å
• α: 90°
• β: 94.531 ± 0.008°
• γ: 90°
• Cell volume: 3177 ± 3 ų
• Cell temperature: 173 K
• Ambient diffraction temperature: 173 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0593
• Residual factor for significantly intense reflections: 0.0485
• Weighted residual factors for significantly intense reflections: 0.1301
• Weighted residual factors for all reflections included in the refinement: 0.1416
• Goodness-of-fit parameter for all reflections included in the refinement: 1.067
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No