Information card for entry 4089072

Structure parameters

• Formula: C48 H54 Cl2 Ge2 N2 P2
• Calculated formula: C48 H54 Cl2 Ge2 N2 P2
• SMILES: [Ge]1([P](c2ccccc2)(N([Ge]([P](c2ccccc2)(N1c1c(C(C)C)cccc1C(C)C)c1ccccc1)Cl)c1c(cccc1C(C)C)C(C)C)c1ccccc1)Cl
• Title of publication: Acyclic α-Phosphinoamido-Germylene: Synthesis and Characterization
• Authors of publication: Pal, Shiv; Dasgupta, Rajarshi; Khan, Shabana
• Journal of publication: Organometallics
• Year of publication: 2016
• Journal volume: 35
• Journal issue: 20
• Pages of publication: 3635
• a: 10.559 ± 0.005 Å
• b: 14.185 ± 0.007 Å
• c: 18.025 ± 0.009 Å
• α: 90°
• β: 104.966 ± 0.012°
• γ: 90°
• Cell volume: 2608 ± 2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 7
• Hermann-Mauguin space group symbol: P 1 n 1
• Hall space group symbol: P -2yac
• Residual factor for all reflections: 0.1151
• Residual factor for significantly intense reflections: 0.0684
• Weighted residual factors for significantly intense reflections: 0.1315
• Weighted residual factors for all reflections included in the refinement: 0.1458
• Goodness-of-fit parameter for all reflections included in the refinement: 0.968
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No