Information card for entry 4089073

Structure parameters

• Formula: C48 H54 Ge N2 P2
• Calculated formula: C48 H54 Ge N2 P2
• SMILES: [Ge](N(P(c1ccccc1)c1ccccc1)c1c(C(C)C)cccc1C(C)C)N(P(c1ccccc1)c1ccccc1)c1c(C(C)C)cccc1C(C)C
• Title of publication: Acyclic α-Phosphinoamido-Germylene: Synthesis and Characterization
• Authors of publication: Pal, Shiv; Dasgupta, Rajarshi; Khan, Shabana
• Journal of publication: Organometallics
• Year of publication: 2016
• Journal volume: 35
• Journal issue: 20
• Pages of publication: 3635
• a: 10.754 ± 0.002 Å
• b: 17.66 ± 0.003 Å
• c: 22.507 ± 0.004 Å
• α: 95.526 ± 0.005°
• β: 91.93 ± 0.006°
• γ: 90.621 ± 0.005°
• Cell volume: 4251.7 ± 1.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1447
• Residual factor for significantly intense reflections: 0.0644
• Weighted residual factors for significantly intense reflections: 0.1276
• Weighted residual factors for all reflections included in the refinement: 0.1577
• Goodness-of-fit parameter for all reflections included in the refinement: 1.013
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No