Crystallography Open Database

Information card for entry 4089074

Preview

Coordinates	4089074.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C48 H54 Ge2 N2 O P2
Calculated formula	C48 H54 Ge2 N2 O P2
SMILES	[Ge]12[P](N([Ge]([P](N2c2c(cccc2C(C)C)C(C)C)(c2ccccc2)c2ccccc2)O1)c1c(cccc1C(C)C)C(C)C)(c1ccccc1)c1ccccc1
Title of publication	Acyclic α-Phosphinoamido-Germylene: Synthesis and Characterization
Authors of publication	Pal, Shiv; Dasgupta, Rajarshi; Khan, Shabana
Journal of publication	Organometallics
Year of publication	2016
Journal volume	35
Journal issue	20
Pages of publication	3635
a	9.348 ± 0.005 Å
b	12.975 ± 0.006 Å
c	19.947 ± 0.009 Å
α	105.161 ± 0.012°
β	94.562 ± 0.013°
γ	105.937 ± 0.013°
Cell volume	2215.4 ± 1.9 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0629
Residual factor for significantly intense reflections	0.0414
Weighted residual factors for significantly intense reflections	0.0878
Weighted residual factors for all reflections included in the refinement	0.0957
Goodness-of-fit parameter for all reflections included in the refinement	1.089
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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