Information card for entry 4089322

Structure parameters

• Common name: [Sn{C3H3O(C2H5)}{C(SiMe3)2SiMe2CH2CH2SiMe2C(SiMe3)2}]
• Formula: C25 H60 O Si6 Sn
• Calculated formula: C25 H60 O Si6 Sn
• Title of publication: Reactions of a Highly Crowded Cyclic Stannylene with Iodoalkanes, Enones, and Dienes. Inhibition of Nucleophilic Substitution at Tin(IV) Centers
• Authors of publication: Asadi, Ashrafolmolouk; Eaborn, Colin; Hill, Michael S.; Hitchcock, Peter B.; Meehan, Margaret M.; Smith, J. David
• Journal of publication: Organometallics
• Year of publication: 2002
• Journal volume: 21
• Journal issue: 12
• Pages of publication: 2430
• a: 12.42 ± 0.0004 Å
• b: 13.7856 ± 0.0005 Å
• c: 20.4785 ± 0.0005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3506.27 ± 0.19 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 62
• Hermann-Mauguin space group symbol: P n a m
• Hall space group symbol: -P 2c 2n
• Residual factor for all reflections: 0.0591
• Residual factor for significantly intense reflections: 0.0558
• Weighted residual factors for significantly intense reflections: 0.128
• Weighted residual factors for all reflections included in the refinement: 0.1296
• Goodness-of-fit parameter for all reflections included in the refinement: 1.26
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No