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Information card for entry 4089396
Preview
Coordinates | 4089396.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C26 H49 Cl Fe O2 Si Sn2 |
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Calculated formula | C26 H49 Cl Fe O2 Si Sn2 |
SMILES | [Sn]([Sn](Cl)(C(C)(C)C)C(C)(C)C)([Fe]1234([c]5([cH]4[cH]3[cH]2[cH]15)[Si](C)(C)C)(C#[O])C#[O])(C(C)(C)C)C(C)(C)C |
Title of publication | Reactions of an Iron Chlorodistannane with Hydroxide: Isolation and Structural Characterization of {(η5-Me3SiC5H4)Fe(CO)[(SntBu2)2(μ-OH)]···DMAP}, DMAP = 4-(N,N-Dimethylamino)pyridine, a μ-OH-Stannyl(stannylene)‒Iron Complex |
Authors of publication | Sharma, Hemant K.; Metta-Magaña, Alejandro J.; Pannell, Keith H. |
Journal of publication | Organometallics |
Year of publication | 2013 |
Journal volume | 32 |
Journal issue | 21 |
Pages of publication | 6218 |
a | 17.063 ± 0.002 Å |
b | 13.201 ± 0.0018 Å |
c | 33.212 ± 0.004 Å |
α | 90° |
β | 115.207 ± 0.005° |
γ | 90° |
Cell volume | 6768.6 ± 1.5 Å3 |
Cell temperature | 296 ± 2 K |
Ambient diffraction temperature | 296 ± 2 K |
Number of distinct elements | 7 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.1014 |
Residual factor for significantly intense reflections | 0.0425 |
Weighted residual factors for significantly intense reflections | 0.1128 |
Weighted residual factors for all reflections included in the refinement | 0.1641 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.894 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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