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Information card for entry 4089398
Preview
Coordinates | 4089398.cif |
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Original paper (by DOI) | HTML |
Formula | C18 H32 Fe O3 Si Sn |
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Calculated formula | C18 H32 Fe O3 Si Sn |
SMILES | [Fe]1234([Sn](O)(C(C)(C)C)C(C)(C)C)([c]5([Si](C)(C)C)[cH]1[cH]2[cH]3[cH]45)(C#[O])C#[O] |
Title of publication | Reactions of an Iron Chlorodistannane with Hydroxide: Isolation and Structural Characterization of {(η5-Me3SiC5H4)Fe(CO)[(SntBu2)2(μ-OH)]···DMAP}, DMAP = 4-(N,N-Dimethylamino)pyridine, a μ-OH-Stannyl(stannylene)‒Iron Complex |
Authors of publication | Sharma, Hemant K.; Metta-Magaña, Alejandro J.; Pannell, Keith H. |
Journal of publication | Organometallics |
Year of publication | 2013 |
Journal volume | 32 |
Journal issue | 21 |
Pages of publication | 6218 |
a | 12.33 ± 0.002 Å |
b | 14.168 ± 0.003 Å |
c | 13.012 ± 0.003 Å |
α | 90° |
β | 102.133 ± 0.003° |
γ | 90° |
Cell volume | 2222.3 ± 0.8 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0799 |
Residual factor for significantly intense reflections | 0.0478 |
Weighted residual factors for significantly intense reflections | 0.1487 |
Weighted residual factors for all reflections included in the refinement | 0.1579 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.134 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4089398.html
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