Information card for entry 4089591

Structure parameters

• Formula: C59 H51 B F24 N3 O4 Rh
• Calculated formula: C59 H51 B F24 N3 O4 Rh
• Title of publication: Cooperative Catalysis: Large Rate Enhancements with Bimetallic Rhodium Complexes
• Authors of publication: Choy, Sandra W. S.; Page, Michael J.; Bhadbhade, Mohan; Messerle, Barbara A.
• Journal of publication: Organometallics
• Year of publication: 2013
• Journal volume: 32
• Journal issue: 17
• Pages of publication: 4726
• a: 17.2065 ± 0.0008 Å
• b: 17.6408 ± 0.001 Å
• c: 19.9732 ± 0.001 Å
• α: 90°
• β: 97.615 ± 0.002°
• γ: 90°
• Cell volume: 6009.1 ± 0.5 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0703
• Residual factor for significantly intense reflections: 0.0513
• Weighted residual factors for significantly intense reflections: 0.1176
• Weighted residual factors for all reflections included in the refinement: 0.1293
• Goodness-of-fit parameter for all reflections included in the refinement: 0.974
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No