Information card for entry 4089592

Structure parameters

• Formula: C45 H23 B F24 N3 O2 Rh
• Calculated formula: C45 H23 B F23.9997 N3 O2 Rh
• Title of publication: Cooperative Catalysis: Large Rate Enhancements with Bimetallic Rhodium Complexes
• Authors of publication: Choy, Sandra W. S.; Page, Michael J.; Bhadbhade, Mohan; Messerle, Barbara A.
• Journal of publication: Organometallics
• Year of publication: 2013
• Journal volume: 32
• Journal issue: 17
• Pages of publication: 4726
• a: 17.0019 ± 0.0007 Å
• b: 13.6347 ± 0.0005 Å
• c: 21.0961 ± 0.0008 Å
• α: 90°
• β: 105.069 ± 0.002°
• γ: 90°
• Cell volume: 4722.2 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0808
• Residual factor for significantly intense reflections: 0.0692
• Weighted residual factors for significantly intense reflections: 0.17
• Weighted residual factors for all reflections included in the refinement: 0.182
• Goodness-of-fit parameter for all reflections included in the refinement: 1.024
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No