Information card for entry 4089651

Structure parameters

• Formula: C48 H76 B2 Li2 O4 P2 Si2
• Calculated formula: C48 H76 B2 Li2 O4 P2 Si2
• Title of publication: Synthesis and Structural Characterization of Phosphine‒Borane-Stabilized Dicarbanions with either Rigid or Flexible Spacers
• Authors of publication: Izod, Keith; Dixon, Casey M.; McMeekin, Emma; Rodgers, Lee; Harrington, Ross W.; Baisch, Ulrich
• Journal of publication: Organometallics
• Year of publication: 2013
• Journal volume: 33
• Journal issue: 1
• Pages of publication: 378
• a: 10.3857 ± 0.0006 Å
• b: 10.558 ± 0.0006 Å
• c: 13.2588 ± 0.0008 Å
• α: 94.78 ± 0.005°
• β: 104.055 ± 0.005°
• γ: 112.142 ± 0.005°
• Cell volume: 1281.35 ± 0.15 ų
• Cell temperature: 150.15 K
• Ambient diffraction temperature: 150.15 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.073
• Residual factor for significantly intense reflections: 0.0579
• Weighted residual factors for significantly intense reflections: 0.1556
• Weighted residual factors for all reflections included in the refinement: 0.1689
• Goodness-of-fit parameter for all reflections included in the refinement: 1.035
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No