Information card for entry 4089652

Structure parameters

• Formula: C50 H90 B2 K2 N6 P2 Si2
• Calculated formula: C50 H90 B2 K2 N6 P2 Si2
• Title of publication: Synthesis and Structural Characterization of Phosphine‒Borane-Stabilized Dicarbanions with either Rigid or Flexible Spacers
• Authors of publication: Izod, Keith; Dixon, Casey M.; McMeekin, Emma; Rodgers, Lee; Harrington, Ross W.; Baisch, Ulrich
• Journal of publication: Organometallics
• Year of publication: 2013
• Journal volume: 33
• Journal issue: 1
• Pages of publication: 378
• a: 23.4801 ± 0.0012 Å
• b: 48.364 ± 0.004 Å
• c: 10.4193 ± 0.0005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 11832.1 ± 1.3 ų
• Cell temperature: 150.15 K
• Ambient diffraction temperature: 150.15 K
• Number of distinct elements: 7
• Space group number: 43
• Hermann-Mauguin space group symbol: F d d 2
• Hall space group symbol: F 2 -2d
• Residual factor for all reflections: 0.057
• Residual factor for significantly intense reflections: 0.0502
• Weighted residual factors for significantly intense reflections: 0.1194
• Weighted residual factors for all reflections included in the refinement: 0.1245
• Goodness-of-fit parameter for all reflections included in the refinement: 1.056
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No