Information card for entry 4089653

Structure parameters

• Formula: C65.5 H61 B Cl F24 N6 O6 Rh
• Calculated formula: C65.5 H61 B Cl F24 N6 O6 Rh
• Title of publication: Rhodium(I) Complexes of the Conformationally Rigid IBioxMe4 Ligand: Isolation of a Stable Low-Coordinate T-Shaped Complex
• Authors of publication: Chaplin, Adrian B.
• Journal of publication: Organometallics
• Year of publication: 2014
• Journal volume: 33
• Journal issue: 3
• Pages of publication: 624
• a: 14.6083 ± 0.0003 Å
• b: 18.2307 ± 0.0004 Å
• c: 28.3089 ± 0.0005 Å
• α: 99.6629 ± 0.0016°
• β: 91.5109 ± 0.0016°
• γ: 107.281 ± 0.0019°
• Cell volume: 7073.4 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0683
• Residual factor for significantly intense reflections: 0.0507
• Weighted residual factors for significantly intense reflections: 0.1213
• Weighted residual factors for all reflections included in the refinement: 0.1307
• Goodness-of-fit parameter for all reflections included in the refinement: 1.029
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No