Information card for entry 4101836

Structure parameters

• Chemical name: E-1,1,4,4-Tetrakis[bis(trimethylsilyl)methyl]- 1,4-diisopropyl-2-diethylamino-2-tetrasilene
• Formula: C38 H101 N Si12
• Calculated formula: C38 H101 N Si12
• SMILES: [Si](=[SiH]/[Si](C([Si](C)(C)C)[Si](C)(C)C)(C([Si](C)(C)C)[Si](C)(C)C)C(C)C)(\[Si](C([Si](C)(C)C)[Si](C)(C)C)(C([Si](C)(C)C)[Si](C)(C)C)C(C)C)N(CC)CC
• Title of publication: Addition of Amines and Hydroborane to the Disilyne RSi\τbSiR (R = SiiPr[CH(SiMe3)2]2) Giving Amino- and Boryl-Substituted Disilenes
• Authors of publication: Katsuhiko Takeuchi; Masao Ikoshi; Masaaki Ichinohe; Akira Sekiguchi
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2010
• Journal volume: 132
• Pages of publication: 930 - 931
• a: 15.205 ± 0.0005 Å
• b: 11.602 ± 0.0004 Å
• c: 32.716 ± 0.0006 Å
• α: 90°
• β: 95.385 ± 0.002°
• γ: 90°
• Cell volume: 5745.9 ± 0.3 ų
• Cell temperature: 120 ± 0.1 K
• Ambient diffraction temperature: 120 ± 0.1 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0696
• Residual factor for significantly intense reflections: 0.0529
• Weighted residual factors for significantly intense reflections: 0.1392
• Weighted residual factors for all reflections included in the refinement: 0.1504
• Goodness-of-fit parameter for all reflections included in the refinement: 1.007
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No