Information card for entry 4101837

Structure parameters

• Chemical name: trans-1,1,4,4-tetrakis[bis(trimethylsilyl)methyl]- 1,4-diisopropyl-2-(N,N-diphenylamino)-2-tetrasilene
• Formula: C46 H101 N Si12
• Calculated formula: C46 H100 N Si12
• SMILES: [Si](=[SiH][Si](C([Si](C)(C)C)[Si](C)(C)C)(C([Si](C)(C)C)[Si](C)(C)C)C(C)C)([Si](C([Si](C)(C)C)[Si](C)(C)C)(C([Si](C)(C)C)[Si](C)(C)C)C(C)C)N(c1ccccc1)c1ccccc1
• Title of publication: Addition of Amines and Hydroborane to the Disilyne RSi\τbSiR (R = SiiPr[CH(SiMe3)2]2) Giving Amino- and Boryl-Substituted Disilenes
• Authors of publication: Katsuhiko Takeuchi; Masao Ikoshi; Masaaki Ichinohe; Akira Sekiguchi
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2010
• Journal volume: 132
• Pages of publication: 930 - 931
• a: 20.579 ± 0.0009 Å
• b: 17.723 ± 0.0006 Å
• c: 19.808 ± 0.0008 Å
• α: 90°
• β: 119.906 ± 0.002°
• γ: 90°
• Cell volume: 6262.4 ± 0.4 ų
• Cell temperature: 150 ± 0.1 K
• Ambient diffraction temperature: 150 ± 0.1 K
• Number of distinct elements: 4
• Space group number: 9
• Hermann-Mauguin space group symbol: C 1 c 1
• Hall space group symbol: C -2yc
• Residual factor for all reflections: 0.0543
• Residual factor for significantly intense reflections: 0.0447
• Weighted residual factors for significantly intense reflections: 0.1188
• Weighted residual factors for all reflections included in the refinement: 0.1239
• Goodness-of-fit parameter for all reflections included in the refinement: 1.056
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No