Information card for entry 4102173

Structure parameters

• Formula: C20 H35 Hf P Si2
• Calculated formula: C20 H35 Hf P Si2
• Title of publication: Si-H Bond Activation of Alkynylsilanes by Group 4 Metallocene Complexes
• Authors of publication: Martin Lamač; Anke Spannenberg; Wolfgang Baumann; Haijun Jiao; Christine Fischer; Sven Hansen; Perdita Arndt; Uwe Rosenthal
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2010
• Journal volume: 132
• Pages of publication: 4369 - 4380
• a: 16.8109 ± 0.0005 Å
• b: 10.2196 ± 0.0003 Å
• c: 14.9047 ± 0.0005 Å
• α: 90°
• β: 109.929 ± 0.002°
• γ: 90°
• Cell volume: 2407.3 ± 0.13 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.066
• Residual factor for significantly intense reflections: 0.0363
• Weighted residual factors for significantly intense reflections: 0.0652
• Weighted residual factors for all reflections included in the refinement: 0.0697
• Goodness-of-fit parameter for all reflections included in the refinement: 0.972
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No