Crystallography Open Database

Information card for entry 4102172

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Coordinates	4102172.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22 H38 Hf Si4
Calculated formula	C22 H38 Hf Si4
Title of publication	Si-H Bond Activation of Alkynylsilanes by Group 4 Metallocene Complexes
Authors of publication	Martin Lamač; Anke Spannenberg; Wolfgang Baumann; Haijun Jiao; Christine Fischer; Sven Hansen; Perdita Arndt; Uwe Rosenthal
Journal of publication	Journal of the American Chemical Society
Year of publication	2010
Journal volume	132
Pages of publication	4369 - 4380
a	32.0481 ± 0.001 Å
b	9.1762 ± 0.0002 Å
c	20.1421 ± 0.0007 Å
α	90°
β	113.035 ± 0.002°
γ	90°
Cell volume	5451.1 ± 0.3 Å³
Cell temperature	200 ± 2 K
Ambient diffraction temperature	200 ± 2 K
Number of distinct elements	4
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0328
Residual factor for significantly intense reflections	0.0199
Weighted residual factors for significantly intense reflections	0.0416
Weighted residual factors for all reflections included in the refinement	0.0433
Goodness-of-fit parameter for all reflections included in the refinement	0.894
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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