Information card for entry 4102348

Structure parameters

• Formula: C20 H51 B Cl N Os P2
• Calculated formula: C20 H51 B Cl N Os P2
• SMILES: [OsH2]1([H][B]1N(C)C)(Cl)([P](C(C)C)(C(C)C)C(C)C)[P](C(C)C)(C(C)C)C(C)C
• Title of publication: Borinium Cations as σ-B-H Ligands in Osmium Complexes
• Authors of publication: Miguel A. Esteruelas; Francisco J. Fernández-Alvarez; Ana M. López; Malka Mora; Enrique Oñate
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2010
• Journal volume: 132
• Pages of publication: 5600 - 5601
• a: 16.105 ± 0.004 Å
• b: 11.323 ± 0.003 Å
• c: 15.526 ± 0.004 Å
• α: 90°
• β: 107.556 ± 0.005°
• γ: 90°
• Cell volume: 2699.4 ± 1.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0635
• Residual factor for significantly intense reflections: 0.0386
• Weighted residual factors for significantly intense reflections: 0.0784
• Weighted residual factors for all reflections included in the refinement: 0.0861
• Goodness-of-fit parameter for all reflections included in the refinement: 1.004
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No