Information card for entry 4102699

Structure parameters

• Formula: C22 H23 Cl F8 N2 Si
• Calculated formula: C22 H23 Cl F8 N2 Si
• Title of publication: Selective Aromatic C-F and C-H Bond Activation with Silylenes of Different Coordinate Silicon
• Authors of publication: Anukul Jana; Prinson P. Samuel; Gašper Tavčar; Herbert W. Roesky; Carola Schulzke
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2010
• Journal volume: 132
• Pages of publication: 10164 - 10170
• a: 9.785 ± 0.002 Å
• b: 9.976 ± 0.002 Å
• c: 13.842 ± 0.003 Å
• α: 89.57 ± 0.03°
• β: 82.58 ± 0.03°
• γ: 89.18 ± 0.03°
• Cell volume: 1339.7 ± 0.5 ų
• Cell temperature: 133 ± 2 K
• Ambient diffraction temperature: 133 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1125
• Residual factor for significantly intense reflections: 0.0832
• Weighted residual factors for significantly intense reflections: 0.221
• Weighted residual factors for all reflections included in the refinement: 0.2396
• Goodness-of-fit parameter for all reflections included in the refinement: 1.038
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No