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Information card for entry 4102700
Preview
Jmol._Canvas2D (Jmol) "jmolApplet0"[x]
Coordinates | 4102700.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C27 H31 Cl F5 N3 Si |
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Calculated formula | C27 H31 Cl F5 N3 Si |
Title of publication | Selective Aromatic C-F and C-H Bond Activation with Silylenes of Different Coordinate Silicon |
Authors of publication | Anukul Jana; Prinson P. Samuel; Gašper Tavčar; Herbert W. Roesky; Carola Schulzke |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2010 |
Journal volume | 132 |
Pages of publication | 10164 - 10170 |
a | 9.832 ± 0.002 Å |
b | 10.142 ± 0.002 Å |
c | 14.53 ± 0.003 Å |
α | 88.37 ± 0.03° |
β | 88.69 ± 0.03° |
γ | 71.03 ± 0.03° |
Cell volume | 1369.5 ± 0.5 Å3 |
Cell temperature | 133 ± 2 K |
Ambient diffraction temperature | 133 ± 2 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0803 |
Residual factor for significantly intense reflections | 0.055 |
Weighted residual factors for significantly intense reflections | 0.1416 |
Weighted residual factors for all reflections included in the refinement | 0.1493 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.065 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4102700.html
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Users of the data should acknowledge the original authors of the
structural data.