Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 4105035
Preview
Coordinates | 4105035.cif |
---|---|
Original paper (by DOI) | HTML |
Chemical name | (E)-1,2-bis(1,1,3,3,5,5,7,7-octaethyl-s-hydrindacen-4-yl)-2- (2-naphtyl)phosphasilene toluene solvate |
---|---|
Formula | C73 H105 P Si |
Calculated formula | C73 H105 P Si |
Title of publication | π-Conjugated Phosphasilenes Stabilized by Fused-Ring Bulky Groups |
Authors of publication | Baolin Li; Tsukasa Matsuo; Daisuke Hashizume; Hiroyuki Fueno; Kazuyoshi Tanaka; Kohei Tamao |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2009 |
Journal volume | 131 |
Pages of publication | 13222 - 13223 |
a | 11.762 ± 0.004 Å |
b | 16.793 ± 0.006 Å |
c | 17.517 ± 0.006 Å |
α | 114.21 ± 0.007° |
β | 90.569 ± 0.004° |
γ | 94.77 ± 0.003° |
Cell volume | 3141 ± 1.9 Å3 |
Cell temperature | 100 K |
Ambient diffraction temperature | 100 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.1354 |
Residual factor for significantly intense reflections | 0.0784 |
Weighted residual factors for significantly intense reflections | 0.1888 |
Weighted residual factors for all reflections included in the refinement | 0.2391 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.037 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4105035.html
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.