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Information card for entry 4105036
Preview
Coordinates | 4105036.cif |
---|---|
Original paper (by DOI) | HTML |
Chemical name | (E)-1,2-bis(1,1,3,3,5,5,7,7-octaethyl-s-hydrindacen-4-yl)- 2-(2- anthryl)phosphasilene tetrahydrofuran solvate |
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Formula | C74 H107 O P Si |
Calculated formula | C74 H107 O P Si |
Title of publication | π-Conjugated Phosphasilenes Stabilized by Fused-Ring Bulky Groups |
Authors of publication | Baolin Li; Tsukasa Matsuo; Daisuke Hashizume; Hiroyuki Fueno; Kazuyoshi Tanaka; Kohei Tamao |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2009 |
Journal volume | 131 |
Pages of publication | 13222 - 13223 |
a | 13.7835 ± 0.0003 Å |
b | 14.4694 ± 0.0004 Å |
c | 16.12 ± 0.0005 Å |
α | 92.9717 ± 0.0015° |
β | 94.968 ± 0.0011° |
γ | 101.214 ± 0.0011° |
Cell volume | 3133.96 ± 0.15 Å3 |
Cell temperature | 90 K |
Ambient diffraction temperature | 90 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0918 |
Residual factor for significantly intense reflections | 0.0671 |
Weighted residual factors for significantly intense reflections | 0.1868 |
Weighted residual factors for all reflections included in the refinement | 0.2117 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.046 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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