Crystallography Open Database

Information card for entry 4105058

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Coordinates	4105058.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C20 H47 B2 Cl P2
Calculated formula	C20 H47 B2 Cl P2
Title of publication	Ionic-Type Reactivity of 1,3-Dibora-2,4-diphosphoniocyclobutane-1,3-diyls: Regio- and Stereoselective Addition of Hydracids
Authors of publication	Gad Fuks; Nathalie Saffon; Laurent Maron; Guy Bertrand; Didier Bourissou
Journal of publication	Journal of the American Chemical Society
Year of publication	2009
Journal volume	131
Pages of publication	13681 - 13689
a	9.7254 ± 0.0009 Å
b	11.3862 ± 0.0011 Å
c	22.736 ± 0.002 Å
α	92.369 ± 0.002°
β	96.916 ± 0.002°
γ	97.929 ± 0.002°
Cell volume	2471.2 ± 0.4 Å³
Cell temperature	133 ± 2 K
Ambient diffraction temperature	133 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1035
Residual factor for significantly intense reflections	0.0589
Weighted residual factors for significantly intense reflections	0.1283
Weighted residual factors for all reflections included in the refinement	0.1462
Goodness-of-fit parameter for all reflections included in the refinement	1.008
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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