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Information card for entry 4105059
Preview
Coordinates | 4105059.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C44 H86 B4 Cl2 P4 |
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Calculated formula | C44 H86 B4 Cl2 P4 |
Title of publication | Ionic-Type Reactivity of 1,3-Dibora-2,4-diphosphoniocyclobutane-1,3-diyls: Regio- and Stereoselective Addition of Hydracids |
Authors of publication | Gad Fuks; Nathalie Saffon; Laurent Maron; Guy Bertrand; Didier Bourissou |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2009 |
Journal volume | 131 |
Pages of publication | 13681 - 13689 |
a | 13.1771 ± 0.001 Å |
b | 14.2465 ± 0.0011 Å |
c | 14.621 ± 0.0011 Å |
α | 67.428 ± 0.001° |
β | 88.668 ± 0.001° |
γ | 87.489 ± 0.001° |
Cell volume | 2532 ± 0.3 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0552 |
Residual factor for significantly intense reflections | 0.037 |
Weighted residual factors for significantly intense reflections | 0.0864 |
Weighted residual factors for all reflections included in the refinement | 0.0963 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.01 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4105059.html
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Users of the data should acknowledge the original authors of the
structural data.