Crystallography Open Database

Information card for entry 4105060

Preview

Coordinates	4105060.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C25.5 H49 B2 F3 O3 P2 S
Calculated formula	C25.5 H49 B2 F3 O3 P2 S
Title of publication	Ionic-Type Reactivity of 1,3-Dibora-2,4-diphosphoniocyclobutane-1,3-diyls: Regio- and Stereoselective Addition of Hydracids
Authors of publication	Gad Fuks; Nathalie Saffon; Laurent Maron; Guy Bertrand; Didier Bourissou
Journal of publication	Journal of the American Chemical Society
Year of publication	2009
Journal volume	131
Pages of publication	13681 - 13689
a	32.3223 ± 0.001 Å
b	11.0928 ± 0.0004 Å
c	19.4956 ± 0.0006 Å
α	90°
β	114.759 ± 0.002°
γ	90°
Cell volume	6347.5 ± 0.4 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	7
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.1118
Residual factor for significantly intense reflections	0.0483
Weighted residual factors for significantly intense reflections	0.106
Weighted residual factors for all reflections included in the refinement	0.1314
Goodness-of-fit parameter for all reflections included in the refinement	0.943
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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