Information card for entry 4105139

Structure parameters

• Formula: C30 H39 Cl5 F Ga N2 P6
• Calculated formula: C30 H39 Cl5 F Ga N2 P6
• SMILES: [Ga](Cl)([Cl-])(Cl)Cl.P12([P+]3(P4P5P3P45)(N1c1c(C(C)C)cccc1C(C)C)N2c1c(C(C)C)cccc1C(C)C)Cl.c1(ccccc1)F
• Title of publication: Preparation of the [(DippNP)~2~(P~4~)~2~]^2+^-Dication by the Reaction of [DippNPCl]2 and a Lewis Acid with P~4~
• Authors of publication: Michael H. Holthausen; Jan J. Weigand
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2009
• Journal volume: 131
• Pages of publication: 14210 - 14211
• a: 12.3398 ± 0.0008 Å
• b: 12.9936 ± 0.0008 Å
• c: 24.7548 ± 0.0016 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3969.1 ± 0.4 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 1 K
• Number of distinct elements: 7
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0291
• Residual factor for significantly intense reflections: 0.0251
• Weighted residual factors for significantly intense reflections: 0.0608
• Weighted residual factors for all reflections included in the refinement: 0.0626
• Goodness-of-fit parameter for all reflections included in the refinement: 1.036
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No