Information card for entry 4105140

Structure parameters

• Formula: C24 H34 Cl14 Ga4 N2 P10
• Calculated formula: C24 H34 Cl14 Ga4 N2 P10
• SMILES: c1(c(cccc1C(C)C)C(C)C)N1[P+]2(N(c3c(cccc3C(C)C)C(C)C)[P+]31P1P4P3P14)P1P3P2P13.Cl[Ga](Cl)([Cl][Ga](Cl)(Cl)Cl)Cl.Cl[Ga](Cl)(Cl)[Cl][Ga](Cl)(Cl)Cl
• Title of publication: Preparation of the [(DippNP)~2~(P~4~)~2~]^2+^-Dication by the Reaction of [DippNPCl]2 and a Lewis Acid with P~4~
• Authors of publication: Michael H. Holthausen; Jan J. Weigand
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2009
• Journal volume: 131
• Pages of publication: 14210 - 14211
• a: 24.2241 ± 0.0017 Å
• b: 11.4374 ± 0.0008 Å
• c: 21.2238 ± 0.0015 Å
• α: 90°
• β: 115.093 ± 0.001°
• γ: 90°
• Cell volume: 5325.3 ± 0.6 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 1 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0441
• Residual factor for significantly intense reflections: 0.0301
• Weighted residual factors for significantly intense reflections: 0.0691
• Weighted residual factors for all reflections included in the refinement: 0.0745
• Goodness-of-fit parameter for all reflections included in the refinement: 1.022
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No