Information card for entry 4105376

Structure parameters

• Formula: C16 H19 As F3 O3 P S
• Calculated formula: C16 H19 As F3 O3 P S
• Title of publication: Phosphinopnictonium Cations: High Yield and General Preparative Procedures for New Interpnictogen Frameworks Exploiting As→P and Sb→P Coordinate Bonds
• Authors of publication: Eamonn Conrad; Neil Burford; Robert McDonald; Michael J. Ferguson
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2009
• Journal volume: 131
• Pages of publication: 17000 - 17008
• a: 11.7585 ± 0.0008 Å
• b: 12.8289 ± 0.0009 Å
• c: 12.9423 ± 0.0009 Å
• α: 90°
• β: 96.48 ± 0.001°
• γ: 90°
• Cell volume: 1939.9 ± 0.2 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0428
• Residual factor for significantly intense reflections: 0.0335
• Weighted residual factors for significantly intense reflections: 0.0838
• Weighted residual factors for all reflections included in the refinement: 0.0889
• Goodness-of-fit parameter for all reflections included in the refinement: 1.044
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No