Information card for entry 4105377

Structure parameters

• Formula: C18 H28 Al2 As2 Cl8 P2
• Calculated formula: C18 H28 Al2 As2 Cl8 P2
• Title of publication: Phosphinopnictonium Cations: High Yield and General Preparative Procedures for New Interpnictogen Frameworks Exploiting As→P and Sb→P Coordinate Bonds
• Authors of publication: Eamonn Conrad; Neil Burford; Robert McDonald; Michael J. Ferguson
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2009
• Journal volume: 131
• Pages of publication: 17000 - 17008
• a: 28.143 ± 0.004 Å
• b: 15.696 ± 0.002 Å
• c: 11.3857 ± 0.0015 Å
• α: 90°
• β: 97.8153 ± 0.0017°
• γ: 90°
• Cell volume: 4982.7 ± 1.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0586
• Residual factor for significantly intense reflections: 0.0425
• Weighted residual factors for significantly intense reflections: 0.1026
• Weighted residual factors for all reflections included in the refinement: 0.1104
• Goodness-of-fit parameter for all reflections included in the refinement: 1.047
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No