Information card for entry 4105451

Structure parameters

• Formula: C24 H44 P4
• Calculated formula: C24 H44 P4
• SMILES: C1(CCCCC1)P1P(P(P1C1CCCCC1)C1CCCCC1)C1CCCCC1
• Title of publication: New Synthetic Procedures to Catena-Phosphorus Cations: Preparation and Dissociation of the First cyclo-Phosphino-halophosphonium Salts
• Authors of publication: Jan J. Weigand; Neil Burford; Reagan J. Davidson; T. Stanley Cameron; Patrick Seelheim
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2009
• Journal volume: 131
• Pages of publication: 17943 - 17953
• a: 10.1235 ± 0.0002 Å
• b: 10.1235 ± 0.0002 Å
• c: 12.411 ± 0.0005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1271.94 ± 0.06 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 1 K
• Number of distinct elements: 3
• Space group number: 114
• Hermann-Mauguin space group symbol: P -4 21 c
• Hall space group symbol: P -4 2n
• Residual factor for all reflections: 0.0222
• Residual factor for significantly intense reflections: 0.0213
• Weighted residual factors for significantly intense reflections: 0.0573
• Weighted residual factors for all reflections included in the refinement: 0.0583
• Goodness-of-fit parameter for all reflections included in the refinement: 1.112
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No