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Information card for entry 4105454
Preview
Coordinates | 4105454.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C12 H27 Cl8 Ga2 P3 |
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Calculated formula | C12 H27 Cl8 Ga2 P3 |
SMILES | P1([P+](CC[P+]1(C)C)(C)C)C1CCCCC1.[Ga]([Cl-])(Cl)(Cl)Cl.[Ga](Cl)(Cl)([Cl-])Cl |
Title of publication | New Synthetic Procedures to Catena-Phosphorus Cations: Preparation and Dissociation of the First cyclo-Phosphino-halophosphonium Salts |
Authors of publication | Jan J. Weigand; Neil Burford; Reagan J. Davidson; T. Stanley Cameron; Patrick Seelheim |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2009 |
Journal volume | 131 |
Pages of publication | 17943 - 17953 |
a | 12.2913 ± 0.0004 Å |
b | 14.8034 ± 0.0005 Å |
c | 14.9881 ± 0.0006 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 2727.13 ± 0.17 Å3 |
Cell temperature | 153 ± 2 K |
Ambient diffraction temperature | 153 ± 1 K |
Number of distinct elements | 5 |
Space group number | 29 |
Hermann-Mauguin space group symbol | P c a 21 |
Hall space group symbol | P 2c -2ac |
Residual factor for all reflections | 0.0298 |
Residual factor for significantly intense reflections | 0.0259 |
Weighted residual factors for significantly intense reflections | 0.0562 |
Weighted residual factors for all reflections included in the refinement | 0.0579 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.026 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4105454.html
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