Crystallography Open Database

Information card for entry 4105455

Preview

Coordinates	4105455.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24.5 H45 Cl Ga I5 P4
Calculated formula	C24.5 H45 Cl Ga I5 P4
Title of publication	New Synthetic Procedures to Catena-Phosphorus Cations: Preparation and Dissociation of the First cyclo-Phosphino-halophosphonium Salts
Authors of publication	Jan J. Weigand; Neil Burford; Reagan J. Davidson; T. Stanley Cameron; Patrick Seelheim
Journal of publication	Journal of the American Chemical Society
Year of publication	2009
Journal volume	131
Pages of publication	17943 - 17953
a	10.5502 ± 0.0003 Å
b	13.5437 ± 0.0005 Å
c	13.9971 ± 0.0005 Å
α	101.395 ± 0.0017°
β	93.704 ± 0.0012°
γ	99.35 ± 0.0016°
Cell volume	1924.86 ± 0.11 Å³
Cell temperature	123.1 K
Ambient diffraction temperature	123.1 ± 0.2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for significantly intense reflections	0.0258
Weighted residual factors for all reflections included in the refinement	0.0305
Goodness-of-fit parameter for all reflections included in the refinement	1.077
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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