Information card for entry 4106625

Structure parameters

• Formula: C16 H40 Cl P Si4
• Calculated formula: C16 H40 Cl P Si4
• SMILES: P1(Cl)C(CCC1([Si](C)(C)C)[Si](C)(C)C)([Si](C)(C)C)[Si](C)(C)C
• Title of publication: A Stable Dialkylphosphinyl Radical
• Authors of publication: Shintaro Ishida; Fumiya Hirakawa; Takeaki Iwamoto
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2011
• Journal volume: 133
• Pages of publication: 12968 - 12971
• a: 6.832 ± 0.0006 Å
• b: 21.5855 ± 0.0018 Å
• c: 16.0108 ± 0.0014 Å
• α: 90°
• β: 93.395 ± 0.001°
• γ: 90°
• Cell volume: 2357 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0405
• Residual factor for significantly intense reflections: 0.0386
• Weighted residual factors for significantly intense reflections: 0.0969
• Weighted residual factors for all reflections included in the refinement: 0.0981
• Goodness-of-fit parameter for all reflections included in the refinement: 1.157
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No