Information card for entry 4106626

Structure parameters

• Formula: C16 H41 P Si4
• Calculated formula: C16 H41 P Si4
• Title of publication: A Stable Dialkylphosphinyl Radical
• Authors of publication: Shintaro Ishida; Fumiya Hirakawa; Takeaki Iwamoto
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2011
• Journal volume: 133
• Pages of publication: 12968 - 12971
• a: 11.3757 ± 0.0019 Å
• b: 12.764 ± 0.002 Å
• c: 16.481 ± 0.003 Å
• α: 90°
• β: 100.954 ± 0.002°
• γ: 90°
• Cell volume: 2349.4 ± 0.7 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0327
• Residual factor for significantly intense reflections: 0.0291
• Weighted residual factors for significantly intense reflections: 0.0765
• Weighted residual factors for all reflections included in the refinement: 0.0805
• Goodness-of-fit parameter for all reflections included in the refinement: 1.043
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No