Crystallography Open Database

Information card for entry 4106761

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Coordinates	4106761.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C60 H144 Ho2 K N6 O12 Si8
Calculated formula	C60 H144 Ho2 K N6 O12 Si8
Title of publication	A N23-Radical-Bridged Terbium Complex Exhibiting Magnetic Hysteresis at 14 K
Authors of publication	Jeffrey D. Rinehart; Ming Fang; William J. Evans; Jeffrey R. Long
Journal of publication	Journal of the American Chemical Society
Year of publication	2011
Journal volume	133
Pages of publication	14236 - 14239
a	10.4651 ± 0.0007 Å
b	13.7377 ± 0.0009 Å
c	16.978 ± 0.0012 Å
α	70.4515 ± 0.0007°
β	77.2633 ± 0.0008°
γ	70.8475 ± 0.0007°
Cell volume	2156 ± 0.3 Å³
Cell temperature	143 ± 2 K
Ambient diffraction temperature	143 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0307
Residual factor for significantly intense reflections	0.0239
Weighted residual factors for significantly intense reflections	0.0538
Weighted residual factors for all reflections included in the refinement	0.0564
Goodness-of-fit parameter for all reflections included in the refinement	1.026
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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