Crystallography Open Database

Information card for entry 4106824

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Coordinates	4106824.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H22 B2 F8 N2 Pd2
Calculated formula	C24 H19 B2 F8 N2 Pd2
Title of publication	Oxidative Dinuclear Addition of a PdI-PdI Moiety to Arenes: Generation of μ-η3:η3-Arene-PdII2 Species
Authors of publication	Tetsuro Murahashi; Kohei Takase; Masa-aki Oka; Sensuke Ogoshi
Journal of publication	Journal of the American Chemical Society
Year of publication	2011
Journal volume	133
Pages of publication	14908 - 14911
a	9.643 ± 0.003 Å
b	11.957 ± 0.004 Å
c	13.585 ± 0.004 Å
α	63.325 ± 0.006°
β	81.36 ± 0.006°
γ	69.636 ± 0.005°
Cell volume	1312.1 ± 0.7 Å³
Cell temperature	296 K
Ambient diffraction temperature	296 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for significantly intense reflections	0.0533
Weighted residual factors for all reflections included in the refinement	0.0613
Goodness-of-fit parameter for all reflections included in the refinement	0.96
Diffraction radiation wavelength	0.71075 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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