Information card for entry 4106825

Structure parameters

• Formula: C32.5 H32.5 B2 F8 N4.5 O Pd2
• Calculated formula: C32.5 H28.5 B2 F8 N4.5 O Pd2
• Title of publication: Oxidative Dinuclear Addition of a PdI-PdI Moiety to Arenes: Generation of μ-η3:η3-Arene-PdII2 Species
• Authors of publication: Tetsuro Murahashi; Kohei Takase; Masa-aki Oka; Sensuke Ogoshi
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2011
• Journal volume: 133
• Pages of publication: 14908 - 14911
• a: 10.2184 ± 0.0007 Å
• b: 13.8764 ± 0.001 Å
• c: 25.8461 ± 0.0018 Å
• α: 89.2379 ± 0.0018°
• β: 81.8766 ± 0.0019°
• γ: 78.169 ± 0.0019°
• Cell volume: 3550.5 ± 0.4 ų
• Cell temperature: 123 K
• Ambient diffraction temperature: 123 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.0599
• Weighted residual factors for all reflections included in the refinement: 0.0704
• Goodness-of-fit parameter for all reflections included in the refinement: 1.111
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No