Information card for entry 4106826

Structure parameters

• Formula: C33.5 H30 B2 F8 N4 Pd2
• Calculated formula: C33.5 H26 B2 F8 N4 Pd2
• Title of publication: Oxidative Dinuclear Addition of a PdI-PdI Moiety to Arenes: Generation of μ-η3:η3-Arene-PdII2 Species
• Authors of publication: Tetsuro Murahashi; Kohei Takase; Masa-aki Oka; Sensuke Ogoshi
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2011
• Journal volume: 133
• Pages of publication: 14908 - 14911
• a: 13.4428 ± 0.0005 Å
• b: 24.2164 ± 0.0009 Å
• c: 10.8013 ± 0.0005 Å
• α: 90°
• β: 101.052 ± 0.001°
• γ: 90°
• Cell volume: 3451 ± 0.2 ų
• Cell temperature: 123 K
• Ambient diffraction temperature: 123 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for significantly intense reflections: 0.0455
• Weighted residual factors for all reflections included in the refinement: 0.0607
• Goodness-of-fit parameter for all reflections included in the refinement: 1.362
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No