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Information card for entry 4106945
Preview
Coordinates | 4106945.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C42 H77 Ge N5 P2 Si |
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Calculated formula | C42 H77 Ge N5 P2 Si |
SMILES | [Si]1(N(C(C)(C)C)P3(N1C(C)(C)C)=C([Ge]N(C1=C3[C@@H]2CC[C@H]1C2)c1c(cccc1C(C)C)C(C)C)P(N(C(C)C)C(C)C)N(C(C)C)C(C)C)(C)C.[Si]1(N(C(C)(C)C)P3(N1C(C)(C)C)=C([Ge]N(C1=C3[C@H]2CC[C@@H]1C2)c1c(cccc1C(C)C)C(C)C)P(N(C(C)C)C(C)C)N(C(C)C)C(C)C)(C)C |
Title of publication | Synthesis and Reactivity of a Phosphine-Stabilized Monogermanium Analogue of Alkynes |
Authors of publication | Juliette Berthe; Juan Manuel Garcia; Edgar Ocando; Tsuyoshi Kato; Nathalie Saffon-Merceron; Abel De Cózar; Fernando P. Cossío; Antoine Baceiredo |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2011 |
Journal volume | 133 |
Pages of publication | 15930 - 15933 |
a | 12.0149 ± 0.0004 Å |
b | 13.333 ± 0.0005 Å |
c | 28.4929 ± 0.0009 Å |
α | 90° |
β | 95.319 ± 0.001° |
γ | 90° |
Cell volume | 4544.8 ± 0.3 Å3 |
Cell temperature | 193 ± 2 K |
Ambient diffraction temperature | 193 ± 2 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.055 |
Residual factor for significantly intense reflections | 0.037 |
Weighted residual factors for significantly intense reflections | 0.0887 |
Weighted residual factors for all reflections included in the refinement | 0.0954 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.02 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4106945.html
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Users of the data should acknowledge the original authors of the
structural data.