Crystallography Open Database

Information card for entry 4108617

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Coordinates	4108617.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C58 H78 B2 F24 N P2 Rh
Calculated formula	C58 H78 B2 F24 N P2 Rh
Title of publication	Amine-Borane σ-Complexes of Rhodium. Relevance to the Catalytic Dehydrogenation of Amine-Boranes
Authors of publication	Thomas M. Douglas; Adrian B. Chaplin; Andrew S. Weller
Journal of publication	Journal of the American Chemical Society
Year of publication	2008
Journal volume	130
Pages of publication	14432 - 14433
a	21.0042 ± 0.0003 Å
b	18.2723 ± 0.0003 Å
c	37.9197 ± 0.0007 Å
α	90°
β	102.29 ± 0.0006°
γ	90°
Cell volume	14219.9 ± 0.4 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	7
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.161
Residual factor for significantly intense reflections	0.0862
Weighted residual factors for significantly intense reflections	0.1909
Weighted residual factors for all reflections included in the refinement	0.2212
Goodness-of-fit parameter for all reflections included in the refinement	1.038
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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