Information card for entry 4108618

Structure parameters

• Formula: C60 H82 B3 F24 N2 P2 Rh
• Calculated formula: C60 H82 B3 F24 N2 P2 Rh
• Title of publication: Amine-Borane σ-Complexes of Rhodium. Relevance to the Catalytic Dehydrogenation of Amine-Boranes
• Authors of publication: Thomas M. Douglas; Adrian B. Chaplin; Andrew S. Weller
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2008
• Journal volume: 130
• Pages of publication: 14432 - 14433
• a: 14.2225 ± 0.0002 Å
• b: 50.9939 ± 0.0007 Å
• c: 19.584 ± 0.0003 Å
• α: 90°
• β: 91.5253 ± 0.0007°
• γ: 90°
• Cell volume: 14198.5 ± 0.4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1179
• Residual factor for significantly intense reflections: 0.0685
• Weighted residual factors for significantly intense reflections: 0.1284
• Weighted residual factors for all reflections included in the refinement: 0.1528
• Goodness-of-fit parameter for all reflections included in the refinement: 1.093
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No